Jun
27
2013
Bastian Asmus
Slag samples of a medieval (12th century) copper smelting furnace.
Top left: #21, XPL. Under crossed polarisers the zinc sulphide can be seen as tiny dendrites within the glassy matrix. The other phases are willemite (wlm) and copper (Cu), which is usually asso ciated with the (Zn,Fe,Cu)S phase, an accompanying phase of copper matte at the Huneberg, from which it probably segregates upon solidification. Free iron oxides are seen as dark and much larger dendrites.
Top right: Another section of #21, under plain polarised light. It shows the abundant spinels, the iron oxides and copper inclusions. Most notably it shows the free baryte (brt) inclusion in the slag matrix.
Bottom left: #22, shows more free baryte (brt), together with a lead antimony matte. The long needles are a mixed iron and zinc oxides and are believed to be franklinite (frk?). #104, is rather more affected by corrosion than the other two samples. It shows mainly spinel (sp), free iron oxides and some willemite (wlm). Spinels are in the same order of magnitude than in the other samples.
The colloquial term Schlackologie is used by several German colleagues in the archaeometric sciences when it comes to the analysis and interpretation of mostly metallurgical slags. Literally it would translate to slagology. But why are slags investigated at all and what exactly is slag?
What are slags and what do they consist of?
Slags are by-products of metallurgical or pyro-technological processes and usually remain at the production site as waste product. For example metallurgical smelting slag is usually composed of five separate components:
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3 comments | posted in Archaeometallurgy, General, Science, slag
Jun
27
2013
Bastian Asmus
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Problem: Your microscope is fine working condition, the optics are flawless, but illumination is either dim, brightness is not adjustable or bulbs are hard to come by.
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Custom made LED adapters are used for fitting the LED to your microscope. Upon request we can also do the conversion.
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The Universal LED Controller is able to drive and dim all prevalent LEDs. Brightness may be controlled continuously between 0 and 100 %. Especially the new and powerful LEDs require fine adjustment if they are used in the bright field. To this end the universal LED controller was fitted with switch reduce the maximum power to 160mA, and thus adjusting the brightness in the bright-field is possible with ease. Of course this range may also be set to a different level by the user.
Further the controller features a set of six pre programmed maximum ratings to be able to drive LEDs other than 10W LEDs such as the CREE XM-L, without danger of destroying them.
The controller uses a softstart, i.e. there are no flashes during turning on the LED.
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LED Adapter
- High Power LED illumination retrofit solution
- custom turned and anodised aluminium heatsink
- e.g. for Zeiss illuminator 467040 and Zeiss Illuminator 15
- adapter for for Carl Zeiss Jena illuminators
- adapter for Carl Zeiss Jena Jenaval, Jenamed,…
- for PZO Biolar
- Leitz Laborlux
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- LED: CREE XM-L
- UV /IR / colour LEDs may also be driven
Controller
- Coarse adjustment 0-100 % light output (0-1600mA)
- Fine adjustment is preset to 0 and 10% light output, may be set by the user
- Maximum current may be set to: 1600, 1200, 900, 700, 350, 160 or 50mA
- constant colour throughout the whole range
- LED reaches a maximum of 65ºC under maximum current
- Aluminium die cast enclosure in black, light grey ot hammerite (grey)
- DC in 4,5-12V
- reverse voltage protection
- works well as battery driven device
- designed and made in Germany
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LED Universal Controller 1600 mA
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no comments | tags: retrofitting LED illumination | posted in Analysis, General, Microscopy